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Document ID ca-nt-wasain-2006-02-21 Title Water Sampling Instructions - Collecting the Samples URL unknown Jurisdiction /ca/nt Subdomain(s) Analytical & measurement methods Language en Status completed Analyzed at 2026-04-01 03:10:19.337872+00:00 Relevance Provides standardized protocols for water sampling required for compliance.

Q Qualitative Requirements (24)

Req ID Category Intent Legal Status Name Subdomain(s) Context Conditions Confidence
#Q001operationaloperationalmandatoryEquipment PreparationotherPrior to sampling, ensure you have obtained all the sampling equipment you require, such as the proper bottles, filtration devices, etc.Prior to samplinghigh
#Q002administrativeoperationalrecommendedWater License AvailabilityotherPlease have your water license (if applicable) available before contacting the laboratory to ensure proper bottles are ordered.if applicablehigh
#Q003operationaloperationalmandatoryFlight Schedule VerificationotherCheck your local departure flight schedule to Yellowknife for the day you plan to take your samples.for the day you plan to take your sampleshigh
#Q004operationaloperationalrecommendedSample Shipping TimingotherSamples should be shipped to the Laboratory as soon as possible after collection. Time your sampling so that the samples can be shipped out by plane as soon as possible.high
#Q005monitoringoperationalmandatoryBottle-Specific InstructionsotherFollow the sampling instructions on the back of this sheet for each bottle type. Package bottles in a cooler and send to the laboratory.high
#Q006reportingreportingmandatoryMicrobiological Test NotificationotherIf your require microbiological tests, such as Total Coliforms, E. coli., Fecal Coliforms, BOD, etc., please contact the laboratory with the collection date and time, the Airline name, the waybill number and the expected time of arrival.If your require microbiological testshigh
#Q007operationalhealthmandatoryGlove UsageotherWear appropriate gloves when collecting any sample to avoid contamination and possible exposure to unhealthy substances.when collecting any samplehigh
#Q008corrective_actionhealthmandatoryPreservative Spill ResponseotherIf you should spill any on your skin or clothes, rinse the area immediately with lots of cool water.If you should spill any on your skin or clotheshigh
#Q009corrective_actionhealthmandatoryMedical Attention for BurnsotherCall a doctor should the burning sensation continue.should the burning sensation continuehigh
#Q010monitoringoperationalmandatoryNutrients Sampling ProcedureotherParameter Group: Nutrients | Preservative: Keep cool at 4 o C | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to top and cap bottle.When sampling for Nutrientshigh
#Q011monitoringoperationalmandatoryBiochemical Oxygen Demand (BOD) Sampling ProcedureotherParameter Group: Biochemical Oxygen Demand (BOD) | Preservative: Keep cool at 4 o C | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to top and cap bottle. 3. Sample must be sent to laboratory within 24 hoursWhen sampling for BODhigh
#Q012monitoringoperationalmandatoryMicrobiological Sampling ProcedureotherParameter Group: Microbiological | Preservative: Sodium thiosulphate and Keep cool at 4 o C | Instructions: 1. DO NOT RINSE BOTTLE 2. Fill to top and cap bottle. 3. Sample must be sent to laboratory within 24 hoursWhen sampling for Microbiological parametershigh
#Q013monitoringoperationalmandatoryTotal Metals Sampling ProcedureotherParameter Group: Total Metals | Preservative: 5mL of 1:3 nitric acid in RED-dot vials | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Total Metalshigh
#Q014monitoringoperationalmandatoryDissolved Metals Sampling ProcedureotherParameter Group: Dissolved Metals | Preservative: 5mL of 1:3 nitric acid in RED-dot vials | Instructions: 2. Rinse bottle three (3) times with filtrate 3. Fill to near the top. 4. Add contents of preservative vialWhen sampling for Dissolved Metalshigh
#Q015monitoringoperationalmandatoryHexane Extractable Material (HEM) Sampling ProcedureotherParameter Group: Hexane Extractable Material (HEM) (also known as Oil and Grease) | Preservative: 4mL 1:1 sulphuric acid in YELLOW-dot vial | Instructions: 2. Fill to shoulder of bottle. 3. Add contents of preservative vialWhen sampling for HEM / Oil and Greasehigh
#Q016monitoringoperationalmandatoryBTEX, THM & Purgeable Hydrocarbons Sampling ProcedureotherParameter Group: BTEX, THM & Purgeable Hydrocarbons | Preservative: Keep cool at 4 o C | Instructions: 1. DO NOT RINSE BOTTLE 2. Fill bottle completely leaving NOWhen sampling for BTEX, THM & Purgeable Hydrocarbonshigh
#Q017monitoringoperationalmandatoryExtractable Hydrocarbons Sampling ProcedureotherParameter Group: Extractable Hydrocarbons | Preservative: Keep cool at 4 o C | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Extractable Hydrocarbonshigh
#Q018monitoringoperationalmandatoryCyanide Sampling ProcedureotherParameter Group: Cyanide | Preservative: 1mL of 6N sodium hydroxide | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Cyanidehigh
#Q019monitoringoperationalmandatoryThiocyanate Sampling ProcedureotherParameter Group: Thiocyanate | Preservative: 2ml of 25% sulphuric acid | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Thiocyanatehigh
#Q020monitoringoperationalmandatoryPhenol Sampling ProcedureotherParameter Group: Phenol | Preservative: 2mL of 20% sulphuric acid | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Phenolhigh
#Q021monitoringoperationalmandatorySulphide Sampling ProcedureotherParameter Group: Sulphide | Preservative: 2mL of 25% zinc acetate | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Sulphidehigh
#Q022monitoringoperationalmandatoryRadionuclide Sampling ProcedureotherParameter Group: Radionuclide | Preservative: 25mL of 17.5% nitric acid | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to near the top. 3. Add contents of preservative vial 4. Cap bottle and mix.When sampling for Radionuclidehigh
#Q023monitoringoperationalmandatoryChlorophyll A Sampling ProcedureotherParameter Group: Chlorophyll A | Preservative: Keep cool at 4 o C | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to top and cap bottle. 3. Sample must be sent to laboratory within 24 hoursWhen sampling for Chlorophyll Ahigh
#Q024monitoringoperationalmandatoryGeneral Chemistry (GREEN) Sampling ProcedureotherParameter Group:  | Marking: GREEN | Preservative: Keep cool at 4 o C | Instructions: 1. Rinse bottle three (3) times with sample 2. Fill to top and cap bottle.When sampling for General Chemistry (GREEN)high

P Quantitative Requirements (29)

Req ID Category Intent Legal Status Name Subdomain(s) Limit Type Limit Value Context Conditions Confidence
#P001operationaloperationalmandatoryNutrients Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CNutrientshigh
#P002operationaloperationalmandatoryBiochemical Oxygen Demand (BOD) Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CBiochemical Oxygen Demand (BOD)high
#P003operationaloperationalmandatoryMicrobiological Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CMicrobiologicalhigh
#P004operationaloperationalmandatoryTotal Metals Preservative Volumeotherrequirement5 mL5mL of 1:3 nitric acid in RED-dot vialsTotal Metalshigh
#P005operationaloperationalmandatoryDissolved Metals Preservative Volumeotherrequirement5 mL5mL of 1:3 nitric acid in RED-dot vialsDissolved Metalshigh
#P006operationaloperationalmandatoryHexane Extractable Material Preservative Volumeotherrequirement4 mL4mL 1:1 sulphuric acid in YELLOW-dot vialHexane Extractable Material (HEM) (also known as Oil and Grease)high
#P007operationaloperationalmandatoryBTEX, THM & Purgeable Hydrocarbons Sample Bottle Volumeotherrequirement40 mL40 mL CLEAR GLASS W/ WHITE LIDBTEX, THM & Purgeable Hydrocarbonshigh
#P008operationaloperationalmandatoryBTEX, THM & Purgeable Hydrocarbons Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CBTEX, THM & Purgeable Hydrocarbonshigh
#P009operationaloperationalmandatoryExtractable Hydrocarbons Sample Bottle Volumeotherrequirement1 L1 L AMBER GLASS W/ WHITE LIDExtractable Hydrocarbonshigh
#P010operationaloperationalmandatoryExtractable Hydrocarbons Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CExtractable Hydrocarbonshigh
#P011operationaloperationalmandatoryCyanide Preservative Volumeotherrequirement1 mL1mL of 6N sodium hydroxideCyanidehigh
#P012operationaloperationalmandatoryThiocyanate Preservative Volumeotherrequirement2 mL2ml of 25% sulphuric acidThiocyanatehigh
#P013operationaloperationalmandatoryPhenol Preservative Volumeotherrequirement2 mL2mL of 20% sulphuric acidPhenolhigh
#P014operationaloperationalmandatorySulphide Preservative Volumeotherrequirement2 mL2mL of 25% zinc acetateSulphidehigh
#P015operationaloperationalmandatoryRadionuclide Preservative Volumeotherrequirement25 mL25mL of 17.5% nitric acidRadionuclidehigh
#P016operationaloperationalmandatoryChlorophyll A Sample Bottle Volumeotherrequirement1 L1L BROWN PLASTIC BOTTLEChlorophyll Ahigh
#P017operationaloperationalmandatoryChlorophyll A Sample Storage Temperatureotherrequirement4 o CKeep cool at 4 o CChlorophyll Ahigh
#P018operationaloperationalmandatorySample Shipping Timeframe (BOD, Microbiological, Chlorophyll A)drinking water, wastewaterrequirement24 hoursSample must be sent to laboratory within 24 hoursApplies to BOD, Microbiological, and Chlorophyll A parameter groupshigh
#P019operationaloperationalmandatoryStandard Bottle Rinsing Frequencydrinking water, wastewaterrequirement3 timesRinse bottle three (3) times with sampleApplies to all groups except Microbiological and BTEX/THM/Purgeable Hydrocarbonshigh
#P020operationaloperationalmandatoryGeneral (Green Marking) Sample Storage Temperaturedrinking water, wastewaterrequirement4 o CKeep cool at 4 o CGeneral parameters indicated by Green markinghigh
#P021operationaloperationalmandatoryCyanide Preservative Concentrationdrinking water, wastewaterrequirement6 N1mL of 6N sodium hydroxideCyanide parametershigh
#P022operationaloperationalmandatoryThiocyanate Preservative Concentrationdrinking water, wastewaterrequirement25 %2ml of 25% sulphuric acidThiocyanate parametershigh
#P023operationaloperationalmandatoryPhenol Preservative Concentrationdrinking water, wastewaterrequirement20 %2mL of 20% sulphuric acidPhenol parametershigh
#P024operationaloperationalmandatorySulphide Preservative Concentrationdrinking water, wastewaterrequirement25 %2mL of 25% zinc acetateSulphide parametershigh
#P025operationaloperationalmandatoryRadionuclide Preservative Concentrationdrinking water, wastewaterrequirement17.5 %25mL of 17.5% nitric acidRadionuclide parametershigh
#P026chemicaloperationalmandatoryTotal Metals Nitric Acid Preservative Concentrationdrinking water, wastewaterrequirement1:3 ratio5mL of 1:3 nitric acid in RED-dot vialsTotal Metals parameter grouphigh
#P027chemicaloperationalmandatoryDissolved Metals Nitric Acid Preservative Concentrationdrinking water, wastewaterrequirement1:3 ratio5mL of 1:3 nitric acid in RED-dot vialsDissolved Metals parameter grouphigh
#P028chemicaloperationalmandatoryHexane Extractable Material (HEM) Sulphuric Acid Preservative Concentrationdrinking water, wastewaterrequirement1:1 ratio4mL 1:1 sulphuric acid in YELLOW-dot vialHEM (Oil and Grease) parameter grouphigh
#P029operationaloperationalmandatoryStandard Bottle Rinsing Frequencydrinking water, wastewaterrequirement3 timesRinse bottle three (3) times with sampleApplies to all parameter groups except Microbiological, BTEX/THM/Purgeable Hydrocarbons, and Hexane Extractable Material (HEM).high

D Definitions (0)

No definitions.